:在r—氧化鋁催化劑上,甲醇氯化合成甲胺的反應(yīng)在下列條件范圍——甲醇與氨之比為1:1～2(摩爾比),反應(yīng)溫度400～440℃、氣態(tài)空速為2000～8000小時,氣體線速0.715～3.02厘米/秒,催化劑粒度14～60目,該反應(yīng)系處于動力學(xué)控制區(qū)域內(nèi)。
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浩瀚色譜使用蒸餾-氣相色譜法測定循環(huán)水中氨、甲胺及甲醇的濃度,及時查出生產(chǎn)系統(tǒng)出現(xiàn)的問題。實驗證明本方法準確、快速、操作簡單,可以在相關(guān)行業(yè)推廣運用。
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名稱：甲胺填充柱
型號：HH-AM
規(guī)格：3m*3mm，60-80目
*高使用溫度：120°C
編號：20240227001
應(yīng)用：工業(yè)甲胺，二甲胺，三甲胺的測定? 氣相色譜法
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On the r-alumina catalyst, the reaction of methanol chlorination to synthesize methylamine is carried out under the following conditions: a ratio of methanol to ammonia of 1:1 to 2 (molar ratio), a reaction temperature of 400 to 440 ℃, a gaseous space velocity of 2000 to 8000 hours, a gas linear velocity of 0.715 to 3.02 cm/s, and a catalyst particle size of 14-60 mesh. The reaction system is within the kinetic control region.
Haohan chromatography uses distillation gas chromatography to determine the concentrations of ammonia, methylamine, and methanol in circulating water, and promptly identifies problems in the production system. The experiment proves that this method is accurate, fast, and easy to operate, and can be promoted and applied in related industries.
Name: Methylamine filled column
Model: HH-AM
Specification: 3m * 3mm, 60-80 mesh
*High operating temperature: 120 ° C
Number: 20240227001
Application: Determination of industrial methylamine, dimethylamine, and trimethylamine by gas chromatography
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